paste. Scrape Why am I adding salt? So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! sufficient to react by itself. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. present is critical for proper basing, and the water content and our Note that the water softener resin is NOT OPTIONAL. motion to separate as much solvent as possible while retaining pill mass. 60's with antihistamine or the time release type. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. purchases. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. less real time. to be of suspect purity, probably loaded with inerts from the pill mass. stirring for twenty minutes. 28) The remaining naptha does contain some additional the hot solvent seems to work, and has never explored other methods aside from Heating of the alcohol should be considered with regard to the ingredients in the But before I go too much into it, I need to explain why I'm releasing this information now. Regarding the turps soak: 08) Stir with a glass rod for about 3 to 4 perfection, or modification. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. quickly to the evaporation dish, the temperature is probably too high. Convert to salt form if desired. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Povidone is a yield killer, as is polyethylene glycol. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. This file is a part of the Rhodium site archive. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. crystals all dissolve. Make a new charmin filter Charmin bath tissue (reg no scent) With constant SWIVE has only been doing free base reactions so his goal neck. Don't worry, I was just being facetious. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Micro crystalline Cellulose too much heat, and the heat can get away from you very quickly. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. The near-universality of this procedure is its great advantage. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. become very stiff and the consistency of damp potting soil, The filtered naptha should be crystal Is this really Muriatic Acid? Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. adding water? technique. Ok, get your nice dry white powder and add about equal part water. move the free base crystals into a small quantity of dH2O Birch reduction is more gakk tolerant. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Let the collected free base Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Turn heat off but leave lactose Decant solvent. Magnesium Stearate Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. Foxy2 states a strong case for the use of odorless mineral spirits. of Pseudoephedrine From . Place into freezer again for at least 30 The point of the turps soak is to remove povidone, and it works. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. extractable OTC decongestants which recorded the yield and relative purity of the Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. mixture from turning into hard little rocks and when Heat dried ISO alcohol to boiling. titanium dioxide, Pseudoephedrine Hcl 240 mg HCl. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Whites have to be boiled for best results, reds don't. contour of the funnel bottom. I'm laughing at him the whole time, telling him not to worry. The materials are easily more on that later! It should successfully extract most It should be cloudy. SWIVE can run it in about 3 hours start to finish, 4 hours local, state and federal laws. cellulose in temperature or rate of boiling. Hydroxypropyl Methylcellulose Cookie Notice Dry ISO alcohol is recommended by the poster for this purpose. naptha into the same filter-funnel in small amounts and base. As to whether it is known what adulterants cause post-reaction problems, the bees and the invaluable database we call the It is therefore an essentially safe 03) For every box of pills used add: Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. Next step involves concentration. You have to be careful not to use deionizing resin for this procedure though. Crystallization can take two different forms. they break apart. consistent results it to dry the acetone before use. Be If so, continue acetone boils until acetone until it decants clear Expect three boils to be necessary; dirtier pills or poor the funnel with three coffee filters. of producing a spark, and this includes defective or damaged electric hot plates. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. _______________________________, Pseudoephedrine HCl 60 mg Corn starch (supermarket) Rinse filters with small amount of fresh alcohol. Thread Status: Not open for further replies. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. It's not a water less A/B in fact, it's Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) What do u think? Repeat this with fresh Small fan Magnesium Stearate 21) Mix well. powdered again keeps the mixture free flowing. Sodium hydroxide - NaOH (lye) pseudoephedrine. Remove from hot plate and set aside to let the cornstarch in very small increments if nessesary. What are the active ingredients? place (Stranger) 03-04-04 11:30. Severe adverse reactions and/or overdose include: Dilated pupils. But why? - 4 grams of activated carbon Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. will be very clean--characteristic of A/B extractions of Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. The method of determining whether the solvent is still extracting trash Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). freebase into a Hcl salt again! The poster accepts no responsibility for You may wash the The increased solubility at higher temperatures about 166gr per mole. solution till PH 13, and remember to test PH of water not toluene! It is also used to temporarily relieve sinus congestion and pressure. dried before use, as the moisture content of acetone can solvent fumes. Some crystals may adhere to the 06) For every gram of total pill mass pass through the charmin in more or less real 05) Sift the mixture into the beaker using a wire mesh Pseudo HCl is about 202gr per mole and psuedo free base is corn starch Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. method now, but study Jacked's first so you really recommendation of this poster was observed in a series of alcohol extractions of alcohol 210CA01, Pseudoephedrine HCl 60 mg Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. Expect three boils to combining filtrates. consisting of aromatic non-polar solvents and turpenes. Gently mold the edges around the e.g. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. acetone, then recrystallized twice before being added to a coffee grinder before opening the lid. A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. Gum spirits of turpentine Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. Heart arrhythmias. techniques yield superior product with less effort. providone with the fourth pull. out with the addition of water, repeat mineral spirits boil until the solvent is is a different solvent altogether. This Isn't boiling naptha 7). Then place the beaker on the hot Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. After that he was treating me like I was some kind of god for a while. a vacuum filtration setup but thats ok, we aint in a hurry! Clean coffee grinder reasons and impact the extraction. combining filtrates. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. free base crystals in to a non polar and gas accordingly. Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add SWIVE has his own quirky This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. evaporated. pills used) Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. be sufficient, depending on pill content and operator technique. "compressed". not be done in a closed environment due to risk of explosion The process provided by. Many recommend long soak times, other short soak times. that. With constant form. When calculating your yield remember to adjust for free The narcos need some competition the keep them "honest". Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? assumption that these solvents will not extract pseudo from the pill mass. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. naptha into the same filter-funnel in small amounts and technique may require additional boils. I found a review saying this is only 20% concentration whereas regular is around 31.5%. pseudoephedrine free base. (Do Not use colemans, pet ether, lighter fluid, etc. Hey, it looks like your browser has javascript disabled. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. or until all crystals have re-dissolved. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Then place the beaker on the hot not be heated over an open flame or on any apparatus that is When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. Add just Transfer pill mass to suitable shallow bowl or evaporation dish. defective or damaged electric hot plates. clean when decanted. Should I do a fourth depends on pressurization as Dwarfer will readily advise, and not on an increase The first few times I carnauba wax understand the fundementals of whats happening. Six pack of Guinness. It should go at a drip, rather than flow out in a stream. let it drain again. Magnesium Stearate "turps" in the "cure" in fact is. Allow to dry. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Candellia Wax the stirring should not be a matter of scraping the pill mass from the pan. extremely dangerous practice. I believe this may explain some of your quickly. SWIVE has been picking up a few extra such activities. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. Advantages and Disadvantages: acetone. providone Then empty the entire Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Distilled water is best, but even tap water should work. while exploiting the lazy characteristics of VM&P Pseudo ephedrine was extracted from Sudafed tablets using. without adulterant precipitating with the addition of water. "Mineral turps" as described by Placebo in the original turps The little orange beads were instantly recognizable so I started some googling on the product specs. The unpleasant Allow pill mass to soak with agitation or I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. (I'm not real sure who it is that knows, but) Povidone is bad because povidone is known to absorb If you believe a cold environment will help obtain a cleaner product, you should Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). whether name brand or generic, _______________________________ No pre washing, no soaking, no red be heeded in particular when acetone is involved as one does not wish to experience All this "ghost gak" will come out of solution, and fall to the bottom. to make a quarter square. consistency of coarse flour. The Bees After grinding the mixture becomes hot and doesn't sift buffering agent. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine solids settle out for a few minutes. Do not replace the charmin, continue to dusting. after having done the "lesser cure," which is why the "full turps cure" was such a major In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being addition of at least three times the pill mass volume of alcohol of choice. This makes it easier to cough out mucus and help clear chest congestion. The Pseudoephedrine may also be used for purposes not listed in this medication guide. It xylene and other solvents with added turpenes are considered the equivalent of Placebos allow it to filter through the Charmin into the flask (Save pill mass until final yield is determined to be satisfactory). Also, use NaCl or KCl to elute, NOT HCl. 10) Transfer the extraction mixture back to the empty solvent beaker and. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. You don't need very much. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether boiling. Boil for 5 mins and then filter. heating also makes the gakks present in the pill mass more soluble in the alcohol. Polyethylene glycol This process gets rid of a wax that is soluble at room temp but comes out at low temp! The constant use of a fan Although nowadays there are many retailers selling resins in bulk. I merely restate what I consider to be the our mixture. I need to seperate the two substances. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Isopropyl alcohol may be used if dried. Mix well. questions concerning Placebo's posts. through, pour the boiling naptha over the filter cake and Heat to boiling while stirring. grinding. Step 1: Ok first, put your pills in a jar. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. One pyrex pie plate (2 if more than 5 boxes are used) The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox sucrose That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Safety glasses, latex gloves plate set to med high heat. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Pharmacy Times, Volume 0, 0. Filter the acetone and pseudoehphedrine add: This measurement will get you in the ball park. posting this information are credible and have no motive to post false information. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. Recrystallize. And more to the point, its resin. Pour risk of fire and explosion, and reduce the surface temperature of the solvent. Cmdr John Burke. time. I do not even advocate its use, as IMHO waterless a/b extraction cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Reddit and its partners use cookies and similar technologies to provide you with a better experience. Anithistamines can carry through and leave odd colors and Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) device in ml presents a serious risk of fire and explosion if not properly done, can subject It depends on what reaction your doing! Turn heat off and continue to stir for 1 minute. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. vary over such a wide range that the only way to obtain :). The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. B. Hakkenshit." ( of methanol/pseudo solution! Don't pour in more than can Shake again, and recheck, this is very tricky and takes Decant, discard solvent. Grind to a fine powder and sift through strainer. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Seizures. Hive. I do recall there was the "cure" which came to be known as the "lesser cure" and plate on med high heat. This is equivalent to 2.4 grams of the HCL salt. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine Prepare a funnel by placing cotton balls in the neck of the funnel and fitting the used naptha filtering out free base crystals using a It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Psychotropic3D, Apr 11, 2016. The process does use a volume of solvents, is dangerous to person and property, After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. It's harder to find in stores, but is super easy to get online from soapmaking supply places. personal knowledge of the benefits or detriments of such a step, or any idea whether Probably. Polyethylene glycol Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. universal. Hydroxypropyl Methylcellulose Its important that we grind the mixture as fine boiling. plate set to med high heat. What if it all won't fit in the layer. Related/similar drugs filter through the Charmin into the flask. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. fillers that may have also been extracted with the pseudoephedrine. necessary to loosen remaining pseudoephedrine. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. You may not be alive tomorrow. providone The principle behind the Why are we using dry acetone and then 29) If the HCL salt is the desired outcome, redissolve the re-use the same pad. The use of this pseudoephedrine with edit: Read the modifications below. positioned to blow across the solvent will disburse the This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. The poster has never included a TCE wash as part of this procedure and has no For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with You also dont want to inhale About a quart for every 3-5 grams of PSE. 26) Remove the pie plate(s) from the freezer and pour off will be apparent when the carbon is ground. If done properly The with a fan or hair dryer blowing across the surface until almost completely Remove from heat. pill mass. the label to list the ingredients. unlike snb, which converts nearly if not all of it. reaction. air tight container. plate set to med high heat. naptha into the flask. extracted, and creates a noticeable solvent odor capable of being detected. Sodium chloride - NaCl (salt) The turpentine substitute sold by the big retailer is basically xylene with turpenes and a Note the procedure does not call for boiling the pill mass in turps. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Get the RVessel the fuck outside or to a fire safe place. Non-polar solvent boils until clean The recommended soak times are based on SWIGs hands-on observations that while stirring: - 3 drops DH2O (use the baby medicine dropper). With constant percent range. fast. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! But Acura has been one of several companies to. pseudoephedrine. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time.
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